TY - JOUR
T1 - Microwave-assisted synthesis of Limonia acidissima Groff gum stabilized palladium nanoparticles for colorimetric glucose sensing
AU - Seku, Kondaiah
AU - Pejjai, Babu
AU - Osman, Ahmed I.
AU - Hussaini, Syed Sulaiman
AU - Al-Abri, Mohammed
AU - Swathi, R.
AU - Hussain, Mushtaq
AU - Kumar, Nadavala Siva
AU - Al-Fatesh, Ahmed S.
AU - Bhagavanth Reddy, G.
N1 - Copyright © 2024 The Author(s). Published by Elsevier Inc. All rights reserved.
PY - 2024/4/1
Y1 - 2024/4/1
N2 - Herein, we present a novel microwave-assisted method for the synthesis of palladium nanoparticles (PdNPs) supported by Limonia acidissima Groff tree extract gum. The synthesized PdNPs were characterized using various analytical techniques, including FTIR, SEM, TEM, UV–visible, and powder XRD analyses. TEM and XRD analysis confirmed that the synthesized LAG-PdNPs are highly crystalline nature spherical shapes with an average size diameter of 7–9 nm. We employed these gum-capped PdNPs to investigate their peroxidase-like activity for colorimetric detection of hydrogen peroxide (H2O2) and glucose. The oxidation of 3,3′,5,5′-tetramethylbenzidine (TMB) by H2O2, catalyzed by PdNPs, produces oxidation products quantified at 652 nm using spectrophotometry. The catalytic activity of PdNPs was optimized with respect to temperature and pH. The developed method exhibited a linear range of detection from 1 to 50 µm, with detection limits of 0.35 µm for H2O2 and 0.60 µm for glucose.
AB - Herein, we present a novel microwave-assisted method for the synthesis of palladium nanoparticles (PdNPs) supported by Limonia acidissima Groff tree extract gum. The synthesized PdNPs were characterized using various analytical techniques, including FTIR, SEM, TEM, UV–visible, and powder XRD analyses. TEM and XRD analysis confirmed that the synthesized LAG-PdNPs are highly crystalline nature spherical shapes with an average size diameter of 7–9 nm. We employed these gum-capped PdNPs to investigate their peroxidase-like activity for colorimetric detection of hydrogen peroxide (H2O2) and glucose. The oxidation of 3,3′,5,5′-tetramethylbenzidine (TMB) by H2O2, catalyzed by PdNPs, produces oxidation products quantified at 652 nm using spectrophotometry. The catalytic activity of PdNPs was optimized with respect to temperature and pH. The developed method exhibited a linear range of detection from 1 to 50 µm, with detection limits of 0.35 µm for H2O2 and 0.60 µm for glucose.
KW - Colorimetric detection
KW - Glucose sensing
KW - Microwave-assisted synthesis
KW - Palladium nanoparticles
UR - http://www.scopus.com/inward/record.url?scp=85182266213&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=85182266213&partnerID=8YFLogxK
UR - https://www.mendeley.com/catalogue/b1c01f7a-49f7-3858-acae-337cb7cf1895/
U2 - 10.1016/j.jcis.2024.01.046
DO - 10.1016/j.jcis.2024.01.046
M3 - Article
C2 - 38211489
AN - SCOPUS:85182266213
SN - 0021-9797
VL - 659
SP - 718
EP - 727
JO - Journal of Colloid and Interface Science
JF - Journal of Colloid and Interface Science
ER -